TY - JOUR
T1 - Reflectance FTIR and SEM characterization of poly[N-vinylcarbazole-co- methylmethacrylate] electrografted carbon fiber surface
T2 - Current density effect
AU - Saraç, A. Sezai
AU - Bismarck, Alexander
AU - Springer, Jürgen
N1 - Funding Information:
The authors would like to thank Jörg Nissen (Zentralein-richtung für Elektronenmikroskopie (ZELMI) of the TU-Berlin) for recording the SEM-micrographs and EDX-spectra, Astrid Müller for performing DSC and FTIR-ATR measurements. The financial support of the DAAD and TUB (Technische Universitat Berlin) is gratefully acknowledged.
PY - 2006/1
Y1 - 2006/1
N2 - Electrografting of poly [N-vinylcarbazole-co-methylmethacrylate] onto high tenacity carbon fiber (TENAX HTA 5000) was carried out under preparative constant current electrolysis conditions by using anode and cathode as fiber towings. The surface morphology of the electrografted carbon fibers was determined by scanning electron microscopy (SEM). FTIR reflectance measurements (FTIR-ATR) were applied for the characterization of chemical composition on the electrografted thin film surface on carbon fiber. The efficiency of the electrocopolymerization on carbon fiber surfaces under preparative constant current electrolysis conditions were evaluated, i.e., current density (charge) vs. thickness, yield and morphology.
AB - Electrografting of poly [N-vinylcarbazole-co-methylmethacrylate] onto high tenacity carbon fiber (TENAX HTA 5000) was carried out under preparative constant current electrolysis conditions by using anode and cathode as fiber towings. The surface morphology of the electrografted carbon fibers was determined by scanning electron microscopy (SEM). FTIR reflectance measurements (FTIR-ATR) were applied for the characterization of chemical composition on the electrografted thin film surface on carbon fiber. The efficiency of the electrocopolymerization on carbon fiber surfaces under preparative constant current electrolysis conditions were evaluated, i.e., current density (charge) vs. thickness, yield and morphology.
UR - https://www.scopus.com/pages/publications/33644499804
U2 - 10.1007/s10853-005-2275-2
DO - 10.1007/s10853-005-2275-2
M3 - Article
AN - SCOPUS:33644499804
SN - 0022-2461
VL - 41
SP - 389
EP - 398
JO - Journal of Materials Science
JF - Journal of Materials Science
IS - 2
ER -