Reflectance FTIR and SEM characterization of poly[N-vinylcarbazole-co- methylmethacrylate] electrografted carbon fiber surface: Current density effect

A. Sezai Saraç; Alexander Bismarck; Jürgen Springer

doi:10.1007/s10853-005-2275-2

Reflectance FTIR and SEM characterization of poly[N-vinylcarbazole-co- methylmethacrylate] electrografted carbon fiber surface: Current density effect

A. Sezai Saraç (Corresponding author), Alexander Bismarck, Jürgen Springer

Publications: Contribution to journal › Article › Peer Reviewed

Abstract

Electrografting of poly [N-vinylcarbazole-co-methylmethacrylate] onto high tenacity carbon fiber (TENAX HTA 5000) was carried out under preparative constant current electrolysis conditions by using anode and cathode as fiber towings. The surface morphology of the electrografted carbon fibers was determined by scanning electron microscopy (SEM). FTIR reflectance measurements (FTIR-ATR) were applied for the characterization of chemical composition on the electrografted thin film surface on carbon fiber. The efficiency of the electrocopolymerization on carbon fiber surfaces under preparative constant current electrolysis conditions were evaluated, i.e., current density (charge) vs. thickness, yield and morphology.

Original language	English
Pages (from-to)	389-398
Number of pages	10
Journal	Journal of Materials Science
Volume	41
Issue number	2
DOIs	https://doi.org/10.1007/s10853-005-2275-2
Publication status	Published - Jan 2006
Externally published	Yes

Funding

The authors would like to thank Jörg Nissen (Zentralein-richtung für Elektronenmikroskopie (ZELMI) of the TU-Berlin) for recording the SEM-micrographs and EDX-spectra, Astrid Müller for performing DSC and FTIR-ATR measurements. The financial support of the DAAD and TUB (Technische Universitat Berlin) is gratefully acknowledged.

Austrian Fields of Science 2012

205019 Material sciences

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10.1007/s10853-005-2275-2

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@article{7ed007dd734047dab343694ceb861af0,

title = "Reflectance FTIR and SEM characterization of poly[N-vinylcarbazole-co- methylmethacrylate] electrografted carbon fiber surface: Current density effect",

abstract = "Electrografting of poly [N-vinylcarbazole-co-methylmethacrylate] onto high tenacity carbon fiber (TENAX HTA 5000) was carried out under preparative constant current electrolysis conditions by using anode and cathode as fiber towings. The surface morphology of the electrografted carbon fibers was determined by scanning electron microscopy (SEM). FTIR reflectance measurements (FTIR-ATR) were applied for the characterization of chemical composition on the electrografted thin film surface on carbon fiber. The efficiency of the electrocopolymerization on carbon fiber surfaces under preparative constant current electrolysis conditions were evaluated, i.e., current density (charge) vs. thickness, yield and morphology.",

author = "Sara{\c c}, \{A. Sezai\} and Alexander Bismarck and J{\"u}rgen Springer",

note = "Funding Information: The authors would like to thank J{\"o}rg Nissen (Zentralein-richtung f{\"u}r Elektronenmikroskopie (ZELMI) of the TU-Berlin) for recording the SEM-micrographs and EDX-spectra, Astrid M{\"u}ller for performing DSC and FTIR-ATR measurements. The financial support of the DAAD and TUB (Technische Universitat Berlin) is gratefully acknowledged.",

year = "2006",

month = jan,

doi = "10.1007/s10853-005-2275-2",

language = "English",

volume = "41",

pages = "389--398",

journal = "Journal of Materials Science",

issn = "0022-2461",

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Reflectance FTIR and SEM characterization of poly[N-vinylcarbazole-co- methylmethacrylate] electrografted carbon fiber surface: Current density effect. / Saraç, A. Sezai (Corresponding author); Bismarck, Alexander; Springer, Jürgen.
In: Journal of Materials Science, Vol. 41, No. 2, 01.2006, p. 389-398.

Publications: Contribution to journal › Article › Peer Reviewed

TY - JOUR

T1 - Reflectance FTIR and SEM characterization of poly[N-vinylcarbazole-co- methylmethacrylate] electrografted carbon fiber surface

T2 - Current density effect

AU - Saraç, A. Sezai

AU - Bismarck, Alexander

AU - Springer, Jürgen

N1 - Funding Information: The authors would like to thank Jörg Nissen (Zentralein-richtung für Elektronenmikroskopie (ZELMI) of the TU-Berlin) for recording the SEM-micrographs and EDX-spectra, Astrid Müller for performing DSC and FTIR-ATR measurements. The financial support of the DAAD and TUB (Technische Universitat Berlin) is gratefully acknowledged.

PY - 2006/1

Y1 - 2006/1

N2 - Electrografting of poly [N-vinylcarbazole-co-methylmethacrylate] onto high tenacity carbon fiber (TENAX HTA 5000) was carried out under preparative constant current electrolysis conditions by using anode and cathode as fiber towings. The surface morphology of the electrografted carbon fibers was determined by scanning electron microscopy (SEM). FTIR reflectance measurements (FTIR-ATR) were applied for the characterization of chemical composition on the electrografted thin film surface on carbon fiber. The efficiency of the electrocopolymerization on carbon fiber surfaces under preparative constant current electrolysis conditions were evaluated, i.e., current density (charge) vs. thickness, yield and morphology.

AB - Electrografting of poly [N-vinylcarbazole-co-methylmethacrylate] onto high tenacity carbon fiber (TENAX HTA 5000) was carried out under preparative constant current electrolysis conditions by using anode and cathode as fiber towings. The surface morphology of the electrografted carbon fibers was determined by scanning electron microscopy (SEM). FTIR reflectance measurements (FTIR-ATR) were applied for the characterization of chemical composition on the electrografted thin film surface on carbon fiber. The efficiency of the electrocopolymerization on carbon fiber surfaces under preparative constant current electrolysis conditions were evaluated, i.e., current density (charge) vs. thickness, yield and morphology.

UR - https://www.scopus.com/pages/publications/33644499804

U2 - 10.1007/s10853-005-2275-2

DO - 10.1007/s10853-005-2275-2

M3 - Article

AN - SCOPUS:33644499804

SN - 0022-2461

VL - 41

SP - 389

EP - 398

JO - Journal of Materials Science

JF - Journal of Materials Science

IS - 2

ER -

Reflectance FTIR and SEM characterization of poly[N-vinylcarbazole-co- methylmethacrylate] electrografted carbon fiber surface: Current density effect

Abstract

Funding

Austrian Fields of Science 2012

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